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J Chromatogr B Analyt Technol Biomed Life Sci

Title:		Volatile composition and enantioselective analysis of chiral terpenoids in Tokaj varietal wines
Author(s):		Furdikova K; Khvalbota L; Machynakova A; Spanik I;
Address:		"Institute of Biotechnology, Faculty of Chemical and Food Technology, Slovak University of Technology in Bratislava, Radlinskeho 9, 812 37 Bratislava, Slovakia. Institute of Analytical Chemistry, Faculty of Chemical and Food Technology, Slovak University of Technology in Bratislava, Radlinskeho 9, 812 37 Bratislava, Slovakia. Institute of Analytical Chemistry, Faculty of Chemical and Food Technology, Slovak University of Technology in Bratislava, Radlinskeho 9, 812 37 Bratislava, Slovakia. Electronic address: ivan.spanik@stuba.sk"
Journal Title:		J Chromatogr B Analyt Technol Biomed Life Sci
Year:		2021
Volume:		20210202
Issue:
Page Number:		122565 -
DOI:		10.1016/j.jchromb.2021.122565
ISSN/ISBN:		1873-376X (Electronic) 1570-0232 (Linking)
Abstract:		"The present work compares VOC profiles of 37 Tokaj varietal wines produced from Furmint, Lipovina and Muskat zlty grape varieties determined by SPME-GC-MS. The identified VOCs underwent treatment using one-way ANOVA and PCA for determination of compounds capable to distinguish wines based on grapevine variety. The presence of high concentration of terpenoids was characteristic for Muskat zlty wines, while Furmint and Lipovina expressed quite high similarity, nevertheless Lipovina was characterized by higher relative concentration of 1,1,6-trimethyl-1,2-dihydronaphtalene. Enantioselective analysis of the dominant terpenoids (limonene, linalool, hotrienol and alpha-terpineol) was performed by heartcut-2D-GC: R form was dominant for limonene and linalool and S enantiomer for hotrienol and alpha-terpineol. Statistical analysis (ANOVA) confirmed R-linalool as the most significant compound responsible for the main differences between studied varietal wines. LDA identified both total linalool and R-linalool as the only significant (p
Keywords:		Gas Chromatography-Mass Spectrometry Hungary Slovakia Solid Phase Microextraction Stereoisomerism *Terpenes/analysis/chemistry Volatile Organic Compounds/analysis/chemistry Wine/*analysis Enantioseparation Multidimensional gas chromatography Terpenoids To;
Notes:		"MedlineFurdikova, Katarina Khvalbota, Liudmyla Machynakova, Andrea Spanik, Ivan eng Netherlands 2021/02/24 J Chromatogr B Analyt Technol Biomed Life Sci. 2021 Mar 15; 1167:122565. doi: 10.1016/j.jchromb.2021.122565. Epub 2021 Feb 2"