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Analyst


Title:A universal temperature controlled membrane interface for the analysis of volatile and semi-volatile organic compounds
Author(s):Creaser CS; Lamarca DG; dos Santos LM; New AP; James PA;
Address:"School of Science, Nottingham Trent University, Clifton Lane, Nottingham, UK NG11 8NS. colin.creaser@ntu.ac.uk"
Journal Title:Analyst
Year:2003
Volume:128
Issue:9
Page Number:1150 - 1156
DOI: 10.1039/b305085h
ISSN/ISBN:0003-2654 (Print) 0003-2654 (Linking)
Abstract:"A universal temperature controlled membrane interface (TCMI) has been constructed for hollow-fibre membranes. The membrane temperature is controllable in the range -70 to 250 degrees C using an electric heater and a flow of cooled nitrogen or helium gas. Volatile and semi-volatile organic compounds may be detected either by continuous diffusion across the membrane or by in-membrane pre-concentration followed by thermal desorption into the detector. The TCMI interface is demonstrated in combination with mass spectrometry and GC-MS, for the determination of VOCs and SVOCs in aqueous and air samples and for the on-line monitoring of a bioreactor"
Keywords:"Flow Injection Analysis/*instrumentation/methods Gas Chromatography-Mass Spectrometry/*methods *Membranes, Artificial Organic Chemicals/*analysis *Temperature;"
Notes:"MedlineCreaser, Colin S Lamarca, David Gomez dos Santos, Luisa M Freitas New, Anthony P James, Phillip A eng Research Support, Non-U.S. Gov't England 2003/10/08 Analyst. 2003 Sep; 128(9):1150-6. doi: 10.1039/b305085h"

 
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