| Title: | Screening of tropical fruit volatile compounds using solid-phase microextraction (SPME) fibers and internally cooled SPME fiber |
| Address: | "Department of Chemistry, University of Waterloo Waterloo, Ontario N2L 3G1, Canada" |
| ISSN/ISBN: | 0021-8561 (Print) 0021-8561 (Linking) |
| Abstract: | "In this study, the optimization and comparison of an internally cooled fiber [cold fiber with polydimethylsiloxane (PDMS) loading] and several commercial solid-phase microextraction (SPME) fibers for the extraction of volatile compounds from tropical fruits were performed. Automated headspace solid-phase microextraction (HS-SPME) using commercial fibers and an internally cooled SPME fiber device coupled to gas chromatography-mass spectrometry (GC-MS) was used to identify the volatile compounds of five tropical fruits. Pulps of yellow passion fruit (Passiflora edulis), cashew (Anacardium occidentale), tamarind (Tamarindus indica L.), acerola (Malphigia glabra L.), and guava (Psidium guajava L.) were sampled. The extraction conditions were optimized using two experimental designs (full factorial design and Doehlert matrix) to analyze the main and secondary effects. The volatile compounds tentatively identified included alcohols, esters, carbonyl compounds, and terpernes. It was found that the cold fiber was the most appropriate fiber for the purpose of extracting volatile compounds from the five fruit pulps studied" |
| Keywords: | Alcohols/analysis Aldehydes/analysis Esters/analysis Fruit/*chemistry Organic Chemicals/*analysis Solid Phase Microextraction/*methods Terpenes/analysis; |
| Notes: | "MedlineCarasek, Eduardo Pawliszyn, Janusz eng Comparative Study Research Support, Non-U.S. Gov't 2006/11/09 J Agric Food Chem. 2006 Nov 15; 54(23):8688-96. doi: 10.1021/jf0613942" |
