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J Chromatogr Sci


Title:Curcumin-Melamine For Solid-Phase Microextraction of Volatile Organic Compounds from Aqueous Samples
Author(s):Mohammadi AA; Davarani SSH; Jafari M; Mehdinia A;
Address:"Department of Chemistry, Shahid Beheshti University, Tehran, Iran. Department of Marine Science, Iranian National Institute for Oceanography and Atmospheric Science, No. 3, Etemadzadeh St., Fatemi Ave., Tehran 1411813389, Iran"
Journal Title:J Chromatogr Sci
Year:2023
Volume:61
Issue:7
Page Number:692 - 698
DOI: 10.1093/chromsci/bmac093
ISSN/ISBN:1945-239X (Electronic) 0021-9665 (Linking)
Abstract:"The hybrid coating of curcumin and melamine was prepared by a simple electrochemical method. Some physical and chemical properties of the fiber were studied by several methods such as FT-IR, scanning electron microscopy and X-ray fluorescence spectroscopy. The fiber was stable at the inlet of a gas chromatograph at temperatures up to 280 degrees C. The fiber has been used for the extraction of ethylbenzene, toluene and xylenes (ETX). Some parameters of headspace solid-phase microextraction, including extraction time, temperature and salt amount, were optimized. Under the optimized situation, the detection limits were 0.15-0.21 mug L -1 and the linear ranges were within the range of 0.5-1,000 mug L-1 (r2 >/= 0.99). The intra-day and inter-day relative standard deviations were 10.2-13.7 and 13.0-15.6%, respectively, at a concentration level of 10 mug L-1 from each compound by applying a single fiber. The method was used to successfully analyze wastewater and pool water samples"
Keywords:
Notes:"PubMed-not-MEDLINEMohammadi, Ali Ahmad Davarani, Saied Saeed Hosseiny Jafari, Mostafa Mehdinia, Ali eng 2022/12/04 J Chromatogr Sci. 2023 Aug 19; 61(7):692-698. doi: 10.1093/chromsci/bmac093"

 
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