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Anal Bioanal Chem


Title:Investigation of cuticular hydrocarbons from Bagrada hilaris genders by SPME/GC-MS
Author(s):De Pasquale C; Guarino S; Peri E; Alonzo G; Colazza S;
Address:"CISAC Department, Universita di Palermo, via Archirafi 38-40, 90123, Palermo, Italy. c.depasquale@unipa.it"
Journal Title:Anal Bioanal Chem
Year:2007
Volume:20070801
Issue:4
Page Number:1259 - 1265
DOI: 10.1007/s00216-007-1503-9
ISSN/ISBN:1618-2642 (Print) 1618-2642 (Linking)
Abstract:"The cuticular hydrocarbons of male and female Bagrada hilaris Burmeister (Heteroptera: Pentatomidae) were investigated, by headspace solid-phase microextraction followed by gas chromatography-mass spectrometry. Measurements were done with fiber coatings of different polarity after optimization of headspace volumes and extraction temperatures. This resulted in the use of polyacrylate fiber, 22-ml vial as the sample holder, and an extraction temperature of 150 degrees C. The analytical procedures allowed identification of 13 peaks, corresponding to a homologous series of n-alkanes (nC(17)-nC(29)). The hydrocarbon profiles of male and female B. hilaris were qualitatively equal, but marked sex-specific quantitative differences were observed for some of the linear alkanes"
Keywords:Acrylic Resins/chemistry Alkanes/*analysis Animals Female *Gas Chromatography-Mass Spectrometry Heteroptera/*chemistry Hydrocarbons/analysis Male Sex Attractants/analysis Sex Factors Solid Phase Extraction/*methods;
Notes:"MedlineDe Pasquale, C Guarino, S Peri, E Alonzo, G Colazza, S eng Germany 2007/08/02 Anal Bioanal Chem. 2007 Oct; 389(4):1259-65. doi: 10.1007/s00216-007-1503-9. Epub 2007 Aug 1"

 
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