Title: | [Rapid determination of 30 volatile organic compounds in workplace air by gas chromatography] |
Address: | "Inspection and Testing Department, Changxing Center for Disease Control and Prevention, Huzhou 313100, China" |
Journal Title: | Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi |
DOI: | 10.3760/cma.j.cn121094-20201217-00697 |
ISSN/ISBN: | 1001-9391 (Print) 1001-9391 (Linking) |
Abstract: | "Objective: To establish a method for rapid detection of DB-WAX capillary column and determination of the workplace air in 30 kinds of volatile organic pollutants. Methods: In August 2020, N-pentane, n-hexane, methylcyclohexane, octane, Acetone, ethyl acetate, butanone, benzene, 3-pentanone, trichloroethylene, tetrachloroethylene, toluene, butyl acetate, 2-hexanone, Isoamyl acetate, ethylbenzene, p-xylene, m-xylene, amyl acetate, o-xylene, chlorobenzene, styrene, cyclohexanone, P-chlorotoluene, bromobenzene, M-dichlorobenzene, p-dichlorobenzene, O-dichlorobenzene, o-Chlorotoluene, 1, 2 , 4-trichlorobenzene of 30 kinds of substances in air were collected by activated carbon tube. After analysis by carbon disulfide, the analytical solution was analyzed by DB-WAX column and determined by FID detector. Results: The above 30 kinds of volatile organic pollutants had good separation effect, the correlation coefficient of the standard curve was above 0.999, the relative standard deviation was 0.1%-3.2%, the desorption efficiency was 77.0%-117.1% , the lower limit of quantitation was 0.33-5.33 mug/ml, and the lowest quantitation concentration was 0.22-3.55 mg/m(3), the recoveries ranged was 95.4%-104.9%. Conclusion: The method can effectively separate and accurately determine 30 volatile organic compounds in these workplaces, and the method is simple and quick" |
Keywords: | "*Air Pollutants, Occupational/analysis Benzene/analysis Chromatography, Gas *Volatile Organic Compounds/analysis Workplace Air Fomites Organic chemicals;" |
Notes: | "MedlineLi, G Qian, M Y Duan, J chi China 2022/04/20 Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi. 2022 Mar 20; 40(3):222-226. doi: 10.3760/cma.j.cn121094-20201217-00697" |