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Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi


Title:[Rapid determination of 30 volatile organic compounds in workplace air by gas chromatography]
Author(s):Li G; Qian MY; Duan J;
Address:"Inspection and Testing Department, Changxing Center for Disease Control and Prevention, Huzhou 313100, China"
Journal Title:Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi
Year:2022
Volume:40
Issue:3
Page Number:222 - 226
DOI: 10.3760/cma.j.cn121094-20201217-00697
ISSN/ISBN:1001-9391 (Print) 1001-9391 (Linking)
Abstract:"Objective: To establish a method for rapid detection of DB-WAX capillary column and determination of the workplace air in 30 kinds of volatile organic pollutants. Methods: In August 2020, N-pentane, n-hexane, methylcyclohexane, octane, Acetone, ethyl acetate, butanone, benzene, 3-pentanone, trichloroethylene, tetrachloroethylene, toluene, butyl acetate, 2-hexanone, Isoamyl acetate, ethylbenzene, p-xylene, m-xylene, amyl acetate, o-xylene, chlorobenzene, styrene, cyclohexanone, P-chlorotoluene, bromobenzene, M-dichlorobenzene, p-dichlorobenzene, O-dichlorobenzene, o-Chlorotoluene, 1, 2 , 4-trichlorobenzene of 30 kinds of substances in air were collected by activated carbon tube. After analysis by carbon disulfide, the analytical solution was analyzed by DB-WAX column and determined by FID detector. Results: The above 30 kinds of volatile organic pollutants had good separation effect, the correlation coefficient of the standard curve was above 0.999, the relative standard deviation was 0.1%-3.2%, the desorption efficiency was 77.0%-117.1% , the lower limit of quantitation was 0.33-5.33 mug/ml, and the lowest quantitation concentration was 0.22-3.55 mg/m(3), the recoveries ranged was 95.4%-104.9%. Conclusion: The method can effectively separate and accurately determine 30 volatile organic compounds in these workplaces, and the method is simple and quick"
Keywords:"*Air Pollutants, Occupational/analysis Benzene/analysis Chromatography, Gas *Volatile Organic Compounds/analysis Workplace Air Fomites Organic chemicals;"
Notes:"MedlineLi, G Qian, M Y Duan, J chi China 2022/04/20 Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi. 2022 Mar 20; 40(3):222-226. doi: 10.3760/cma.j.cn121094-20201217-00697"

 
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