« Previous AbstractEnvironmental fate and biodegradability of benzene derivatives as studied in a model aquatic ecosystem    Next Abstract"Combined removal of a BTEX, TCE, and cis-DCE mixture using Pseudomonas sp. immobilized on scrap tyres" »

Se Pu

Title:		[Determination of 10 volatile organic compounds in toys by headspace gas chromatography-mass spectrometry]
Author(s):		Lu Q; Zhang Q; Kang S; Bai H; Wang C;
Address:		"Institute of Industrial Product Inspection, Chinese Academy of Inspection and Quarantine, Beijing 100123, China"
Journal Title:		Se Pu
Year:		2010
Volume:		28
Issue:		8
Page Number:		800 - 804
DOI:		10.3724/sp.j.1123.2010.00800
ISSN/ISBN:		1000-8713 (Print) 1000-8713 (Linking)
Abstract:		"A headspace gas chromatography-mass spectrometry (HS-GC-MS) method was developed for the determination of 10 residual volatile organic compounds (VOCs) in toys. The experimental conditions such as headspace temperature, headspace time and the analytical conditions of GC-MS were optimized. Toy samples were treated at 140 degrees C for 45 min, and then the evolved products were separated on a DB-624 column, determined by MS and quantified by external standard method. The recoveries were from 79% to 106% and the relative standard deviations (RSDs) were from 0.4% to 5.6%. The linear range was 0.001 - 2.0 microg with a good linear correlation coefficient (r > 0.994 0) and the limits of quantification (LOQ) were less than 0 66 mg/kg. The method is accurate, simple, rapid, and is suitable for the analysis of residual VOCs in various toys"
Keywords:
Notes:		"PubMed-not-MEDLINELu, Qing Zhang, Qing Kang, Suyuan Bai, Hua Wang, Chao chi English Abstract China 2011/01/26 Se Pu. 2010 Aug; 28(8):800-4. doi: 10.3724/sp.j.1123.2010.00800"