| Title: | Preparation and Application of Standardized Typical Volatile Components Fraction from Turmeric (Curcuma longa L.) by Supercritical Fluid Extraction and Step Molecular Distillation |
| Author(s): | Lv GP; Hu DJ; Zhou YQ; Zhang QW; Zhao J; Li SP; |
| Address: | "State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macao 999078, China. guangpinglv2012@hotmail.com. School of Pharmaceutical Sciences, Nanjing Tech University, Nanjing 211800, China. guangpinglv2012@hotmail.com. State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macao 999078, China. hdjred@gmail.com. State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macao 999078, China. yb27511@umac.mo. State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macao 999078, China. QWZhang@umac.mo. State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macao 999078, China. jingzhao@umac.mo. State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macao 999078, China. spli@umac.mo" |
| DOI: | 10.3390/molecules23071831 |
| ISSN/ISBN: | 1420-3049 (Electronic) 1420-3049 (Linking) |
| Abstract: | "A green and reliable method using supercritical fluid extraction (SFE) and molecular distillation (MD) was optimized for the separation and purification of standardized typical volatile components fraction (STVCF) from turmeric to solve the shortage of reference compounds in quality control (QC) of volatile components. A high quality essential oil with 76.0% typical components of turmeric was extracted by SFE. A sequential distillation strategy was performed by MD. The total recovery and purity of prepared STVCF were 97.3% and 90.3%, respectively. Additionally, a strategy, i.e., STVCF-based qualification and quantitative evaluation of major bioactive analytes by multiple calibrated components, was proposed to easily and effectively control the quality of turmeric. Compared with the individual calibration curve method, the STVCF-based quantification method was demonstrated to be credible and was effectively adapted for solving the shortage of reference volatile compounds and improving the QC of typical volatile components in turmeric, especially its functional products" |
| Keywords: | "*Chemical Fractionation/instrumentation/methods Curcuma/*chemistry *Distillation/instrumentation/methods Gas Chromatography-Mass Spectrometry/methods Oils, Volatile/chemistry/isolation & purification Plant Extracts/*chemistry/*isolation & purification Pla;" |
| Notes: | "MedlineLv, Guang-Ping Hu, De-Jun Zhou, Yan-Qing Zhang, Qing-Wen Zhao, Jing Li, Shao-Ping eng Switzerland 2018/07/26 Molecules. 2018 Jul 23; 23(7):1831. doi: 10.3390/molecules23071831" |
