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J Hazard Mater


Title:The characterization and influence factors of semi-volatile compounds from mechanically recycled polyethylene terephthalate (rPET) by combining GCxGC-TOFMS and chemometrics
Author(s):Wu S; Wu X; Li H; Li D; Zheng J; Lin Q; Nerin C; Zhong H; Dong B;
Address:"National Reference Laboratory for Food Contact Material (Guangdong), Guangzhou Customs Technology Center, Guangzhou 510075, China. Key Laboratory of Product Packaging and Logistics, Packaging Engineering Institute, Jinan University, Zhuhai 519070, China. Department of Analytical Chemistry, GUIA Group, I3A, EINA, University of Zaragoza, Maria de Luna 3, 50018 Zaragoza, Spain. National Reference Laboratory for Food Contact Material (Guangdong), Guangzhou Customs Technology Center, Guangzhou 510075, China. Electronic address: marco.zhong@iqtc-fcm.com. National Reference Laboratory for Food Contact Material (Guangdong), Guangzhou Customs Technology Center, Guangzhou 510075, China. Electronic address: dongb@iqtc-fcm.com"
Journal Title:J Hazard Mater
Year:2022
Volume:20220712
Issue:
Page Number:129583 -
DOI: 10.1016/j.jhazmat.2022.129583
ISSN/ISBN:1873-3336 (Electronic) 0304-3894 (Linking)
Abstract:"A non-targeted method was developed for screening the semi-volatile compounds of different mechanically recycled PET intended for food contact materials. The data was further analyzed by multiple chemometrics methods to obtain the difference level, and the potential influence factors were investigated. The results showed that total dissolution with comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry was more effective than other reported methods. Based on the difference level, 97 compounds were characterized into 4 levels. 1-Methyl-2-pyrrolidinone originating from organic solvent was recognized as level IV and could be determined as the primary difference indicator. The contaminant is mainly attributed to the residuum derived from non-food consumer products. The specific types of contaminants and process parameters of the recycling, such as moisture content, properties of rPET, and temperature, were the potential key factors affecting the presence of semi-volatile compounds of mechanically recycled rPET"
Keywords:Chemometrics Gas Chromatography-Mass Spectrometry/methods *Polyethylene Terephthalates/chemistry Recycling *Volatile Organic Compounds/analysis Difference level Influencing factor Rpet Semi-volatile compounds TDs-GCxGC-QTOF-MS;
Notes:"MedlineWu, Siliang Wu, Xuefeng Li, Hanke Li, Dan Zheng, Jianguo Lin, Qinbao Nerin, Cristina Zhong, Huaining Dong, Ben eng Research Support, Non-U.S. Gov't Netherlands 2022/07/26 J Hazard Mater. 2022 Oct 5; 439:129583. doi: 10.1016/j.jhazmat.2022.129583. Epub 2022 Jul 12"

 
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