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J Chem Ecol


Title:"Mass spectral determination of aldehydes, ketones, and carboxylic acids using 1,1-dimethylhydrazine"
Author(s):McDaniel CA; Howard RW;
Address:"United States Department of Agriculture, National Monitoring and Residue Analysis Laboratory Plant Protection and Quarantine, Animal and Plant Health Inspection Service, P.O. Box 3209, 39505-3209, Gulfport, Mississippi"
Journal Title:J Chem Ecol
Year:1985
Volume:11
Issue:3
Page Number:303 - 310
DOI: 10.1007/BF01411416
ISSN/ISBN:0098-0331 (Print) 0098-0331 (Linking)
Abstract:"Analyses of nanogram to milligram quantities of aliphatic aldehydes, fatty acids, and unhindered aliphatic ketones such as those typically found in pheromonal blends have been effected by treating these mixtures with 1,1-dimethylhydrazine. The aldehydes and ketones formN,N-dimethylhydrazones, while the fatty acids form methyl esters. Structural elucidation of the reaction products was achieved using EI and CI gas chromatography-mass spectrometry"
Keywords:
Notes:"PubMed-not-MEDLINEMcDaniel, C A Howard, R W eng 1985/03/01 J Chem Ecol. 1985 Mar; 11(3):303-10. doi: 10.1007/BF01411416"

 
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