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J Sep Sci


Title:Development of a method for the monitoring of odor-causing compounds in atmospheres surrounding wastewater treatment plants
Author(s):Godayol A; Marce RM; Borrull F; Antico E; Sanchez JM;
Address:"Department of Chemistry, Universitat de Girona, Campus Montilivi, Girona, Spain"
Journal Title:J Sep Sci
Year:2013
Volume:36
Issue:9-Oct
Page Number:1621 - 1628
DOI: 10.1002/jssc.201300046
ISSN/ISBN:1615-9314 (Electronic) 1615-9306 (Linking)
Abstract:"This study describes the development of an analytical method based on active collection in a multisorbent Tenax TA/Carbograph 1TD tube, followed by thermal desorption and GC-MS for the determination of 16 volatile organic compounds in air samples. The analyzed compounds include ozone precursors and odor-causing compounds belonging to different chemical families (sulfur- and nitrogen-containing compounds, aldehydes, and terpenes). Two types of sorbents were tested and desorption conditions (temperature, time, and sampling, and desorption flow) were evaluated. External calibration was carried out using the multisorbent bed. Method detection limits in the range 0.2-2.0 mug m(-3) for 1 L samples were obtained. The method was applied for determining the target compounds in air samples from two different wastewater treatment plants. Most compounds were detected and toluene, limonene, and nonanal were found in particularly high concentrations with maximum values of 438, 233, and 382 mug m(-3), respectively"
Keywords:Air Pollutants/*analysis Environmental Monitoring/*methods Gas Chromatography-Mass Spectrometry/*methods Odorants/*analysis Volatile Organic Compounds/*analysis Wastewater/*analysis Water Purification/*instrumentation;
Notes:"MedlineGodayol, Anna Marce, Rosa M Borrull, Francesc Antico, Enriqueta Sanchez, Juan M eng Evaluation Study Research Support, Non-U.S. Gov't Germany 2013/03/16 J Sep Sci. 2013 May; 36(9-10):1621-8. doi: 10.1002/jssc.201300046"

 
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