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Molecules

Title:		Comparison of Phenolic Profile of Balsamic Vinegars Determined Using Liquid and Gas Chromatography Coupled with Mass Spectrometry
Author(s):		Kaspar M; Bajer T; Bajerova P; Cesla P;
Address:		"Department of Analytical Chemistry, Faculty of Chemical Technology, University of Pardubice, Studentska 573, CZ-532 10 Pardubice, Czech Republic"
Journal Title:		Molecules
Year:		2022
Volume:		20220217
Issue:		4
Page Number:		-
DOI:		10.3390/molecules27041356
ISSN/ISBN:		1420-3049 (Electronic) 1420-3049 (Linking)
Abstract:		"Balsamic vinegar is one of the best known and most popular types of vinegar, and it is a rich source of polyphenolic compounds. The quality of balsamic vinegar as well as the content of phenolic substances vary depending on the production method. In the present work, we have developed a method for comprehensive characterization of the content of phenolic compounds in balsamic vinegars based on the combination of gas chromatography (GC) and high-performance liquid chromatography (HPLC) coupled with mass spectrometric detection in single mode (MS) and tandem mode (MS/MS). In total, 14 samples of different types of balsamic vinegar were analyzed without difficulty in sample preparation. The separation conditions and detection parameters of HPLC-MS/MS were optimized and used for the determination of 29 phenolic compounds and 6 phenolic acids. The profile of phenolic compounds was completed by semi-quantitative analysis of volatile organic compounds using GC-MS after optimized headspace solid-phase microextraction. Gallic acid, protocatechuic acid, caffeic acid, and p-coumaric acid have been identified as the major phenolic compounds in balsamic vinegars"
Keywords:		"Acetic Acid/*analysis/*chemistry/isolation & purification Chemical Fractionation *Chromatography, High Pressure Liquid *Gas Chromatography-Mass Spectrometry Phenols/analysis *Tandem Mass Spectrometry antioxidants balsamic vinegar gas chromatography liquid;"
Notes:		"MedlineKaspar, Michal Bajer, Tomas Bajerova, Petra Cesla, Petr eng 18-14893S/Czech Science Foundation/ Switzerland 2022/02/26 Molecules. 2022 Feb 17; 27(4):1356. doi: 10.3390/molecules27041356"