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J Chromatogr Sci


Title:Extraction of Volatile Flavor Compounds From Tobacco Leaf Through a Low-Density Polyethylene Membrane
Author(s):Yokoi M; Shimoda M;
Address:"Tobacco Science Research Center, Japan Tobacco Inc., 6-2, Umegaoka, Aoba-ku, Yokohama227-8512, Japan. Food Process Engineering, Division of Food Science and Technology, Bioresource and Bioenvironmental Science, Kyushu University, 6-10-1, Hakozaki, Higashi-ku, Fukuoka812-8581, Japan"
Journal Title:J Chromatogr Sci
Year:2017
Volume:55
Issue:3
Page Number:373 - 377
DOI: 10.1093/chromsci/bmw178
ISSN/ISBN:1945-239X (Electronic) 0021-9665 (Linking)
Abstract:"A low-density polyethylene (LDPE) membrane pouch method was developed to extract volatile flavor compounds from tobacco leaf. Tobacco leaf suspended in water was enclosed in a pouch prepared from a LDPE membrane of specific gravity 0.92 g/cm3 and 0.03 mm thickness and then extracted with diethyl ether. In comparison with direct solvent extraction, LDPE membrane excluded larger and higher boiling point compounds which could contaminate a gas chromatograph inlet and damage a column. Whilst being more convenient than a reduced-pressure steam distillation, it could extract volatile flavor compounds of wide range of molecular weight and polarity. Repeatabilities in the extracted amounts were ranged from 0.38% of 2.3-bipyridyl to 26% of beta-ionone, and average value of 39 compounds was 5.9%"
Keywords:"Gas Chromatography-Mass Spectrometry Membranes, Artificial Plant Extracts/analysis/chemistry/*isolation & purification Plant Leaves/*chemistry Polyethylene/*chemistry Reproducibility of Results Tobacco/*chemistry Volatile Organic Compounds/analysis/chemis;"
Notes:"MedlineYokoi, Michinori Shimoda, Mitsuya eng 2016/11/25 J Chromatogr Sci. 2017 Mar 1; 55(3):373-377. doi: 10.1093/chromsci/bmw178"

 
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