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Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi


Title:[Simultaneous determination of various volatile organic compounds in urine by headspace GC-MS]
Author(s):Lin YR; Li TD; Liu F; Yun JP; Xie YX; Chen JH;
Address:"Shenzhen Prevention and Treatment center for Occupational Diseases, Shenzhen 518001, China"
Journal Title:Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi
Year:2018
Volume:36
Issue:4
Page Number:305 - 307
DOI: 10.3760/cma.j.issn.1001-9391.2018.04.019
ISSN/ISBN:1001-9391 (Print) 1001-9391 (Linking)
Abstract:"Objective: To establish a method for determination of acetone, dichloromethane, hexane, 1, 1, 1-trichloroethane, 1, 2-dichloroethane, benzene, toluene, ethylbenzene etc organic compounds in urine by headspace gas chromatography-mass spectrometry (GC-MS) . Methods: Headspace gases of urine samples were injected into GC and determined by mass. Results: Determination of urine components were in a good linear range in their concentration range of this method. The correlation coefficients were between 0.996 and 1.000 with the detection limits between 0.1 mug/L and 4.5 mug/L, the precisions were between 1.3% and 4.6%, the recovery rates were between 86.2% and 97.4%. Conclusion: This method has the advantages of low detection limits, high accuracy, high precision and simple pretreatment, which is suitable for the determination of the content of various volatile organic compounds in urine"
Keywords:Benzene Gas Chromatography-Mass Spectrometry/*methods Humans Limit of Detection Toluene Volatile Organic Compounds/chemistry/isolation & purification/*urine Gc-ms Headspace Organic compounds Urine;
Notes:"MedlineLin, Y R Li, T D Liu, F Yun, J P Xie, Y X Chen, J H chi China 2018/07/13 Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi. 2018 Apr 20; 36(4):305-307. doi: 10.3760/cma.j.issn.1001-9391.2018.04.019"

 
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