| Title: | In-needle extraction device designed for gas chromatographic analysis of volatile organic compounds |
| Author(s): | Saito Y; Ueta I; Kotera K; Ogawa M; Wada H; Jinno K; |
| Address: | "School of Materials Science, Toyohashi University of Technology, 1-1 Hibarigaoka, Toyohashi 441-8580, Japan" |
| DOI: | 10.1016/j.chroma.2005.08.048 |
| ISSN/ISBN: | 0021-9673 (Print) 0021-9673 (Linking) |
| Abstract: | "A novel in-needle extraction device has been developed for the preconcentration of gaseous organic compounds prior to the determination in gas chromatography (GC). As the extraction medium, a copolymer of methacrylic acid and ethylene glycol dimethacrylate was synthesized. Based on the results in the preliminary experiments, the desorption conditions such as desorption temperature and time have been optimized along with the evaluation of the extraction efficiency. The storage performance of the needle extraction device was also studied. The results clearly demonstrated the excellent extraction performance for typical organic solvents and also suggested the future possibility such as in the applications for the analysis of working environments" |
| Keywords: | "Chromatography, Gas/*methods Organic Chemicals/*analysis Reference Standards Reproducibility of Results Volatilization;" |
| Notes: | "MedlineSaito, Yoshihiro Ueta, Ikuo Kotera, Kenzo Ogawa, Mitsuhiro Wada, Hiroo Jinno, Kiyokatsu eng Research Support, Non-U.S. Gov't Netherlands 2006/01/31 J Chromatogr A. 2006 Feb 17; 1106(1-2):190-5. doi: 10.1016/j.chroma.2005.08.048. Epub 2005 Sep 2" |
