Title: | Fast analysis of volatile compounds from Lippia citriodora with nanoporous aluminum wire as solid-phase microextraction fibres |
Author(s): | Nemati Kharajuo M; Piryaei M; Babashpour Asl M; Abolghasemi MM; |
Address: | "a Department of Horticulture, College of Agriculture , Islamic Azad University , Maragheh , Iran. b Faculty of Science, Department of Chemistry , University of Maragheh , Maragheh , Iran" |
DOI: | 10.1080/14786419.2016.1233407 |
ISSN/ISBN: | 1478-6427 (Electronic) 1478-6419 (Linking) |
Abstract: | "In this study, the efficiency of nanoporous aluminium wires as fibres for headspace solid-phase microextraction (HS-SPME) of volatile compounds from Lippia citriodora was investigated and compared with two anodised methods. The prepared fibres are durable with very good chemical and thermal stability which can be coupled to GC and GC/MS. A one at-a-time optimisation strategy was applied for optimising the important extraction parameters such as extraction temperature, extraction time, sample mass and added water. Compared with hydrodistillation (HD), HS-SPME provide the advantages of a small amount of sample, time-saving, simplicity and cheapness" |
Keywords: | Aluminum/*chemistry Gas Chromatography-Mass Spectrometry/methods Lippia/*chemistry Nanopores Solid Phase Microextraction/*methods Temperature Time Factors Volatile Organic Compounds/*analysis Lippia citriodora Nanoporous aluminium microextraction; |
Notes: | "MedlineNemati Kharajuo, Mohammad Piryaei, Marzieh Babashpour Asl, Marzieh Abolghasemi, Mir Mahdi eng England 2016/09/23 Nat Prod Res. 2017 Feb; 31(3):351-354. doi: 10.1080/14786419.2016.1233407. Epub 2016 Sep 21" |