Title: | Evaluation of the volatile profile of Tuber liyuanum by HS-SPME with GC-MS |
Address: | "a Agricultural College , Jilin Agriculture University , Changchun , P.R. China. b Branch of Food Engineering , Jilin Business and Technology College , Changchun , P.R. China" |
DOI: | 10.1080/14786419.2016.1253082 |
ISSN/ISBN: | 1478-6427 (Electronic) 1478-6419 (Linking) |
Abstract: | "The volatile components of Tuber liyuanum were determined by HS-SPME with GC-MS for the first time. The effects of different fibre coating, extraction time, extraction temperature and sample amount were studied to get optimal extraction conditions. The optimal conditions were SPME fibre of Carboxen/PDMS, extraction time of 40 min, extraction temperature of 80 degrees C, sample amount of 2 g. Under these conditions 57 compounds in volatile of T. liyuanum were detected with a resemblance percentage above 80%. Aldehydes and aromatics were the main chemical families identified. The contribution of 3-Octanone(11.67%), phenylethyl alcohol (10.60%), isopentana (9.29%) and methylbutana (8.06%) for the total volatile profile were more significant in T. liyuanum than other compounds" |
Keywords: | Aldehydes/analysis Ascomycota/*chemistry China Food Analysis/methods Gas Chromatography-Mass Spectrometry/*methods Ketones/analysis Phenylethyl Alcohol/analysis Solid Phase Microextraction/*methods Temperature Volatile Organic Compounds/*analysis Gc/ms Sp; |
Notes: | "MedlineLiu, Changjiao Li, Yu eng England 2016/11/11 Nat Prod Res. 2017 Apr; 31(8):972-975. doi: 10.1080/14786419.2016.1253082. Epub 2016 Nov 10" |