Title: | Analysis of volatile compounds in some typical Brazilian fruits and juices by SPME-GC method |
Author(s): | de Lourdes Cardeal Z; Guimaraes EM; Parreira FV; |
Address: | "Chemistry Department, ICEx, Federal University of Minas Gerais, Belo Horizonte, M.G. Brazil. zenilda@ufmg.br" |
DOI: | 10.1080/02652030500132893 |
ISSN/ISBN: | 0265-203X (Print) 0265-203X (Linking) |
Abstract: | "This paper describes the analysis of volatile organic compounds (VOC) in typical Brazilian fruit and fruit juices by a solid-phase microextraction (SPME) method using a capillary gas chromatography system with flame ionization detection and mass spectrometry (GC-MS). A SPME holder with a 100-microm polydimethilsiloxane fibre coating was utilized. The optimal conditions were desorption at 220 degrees C for 1 min, absorption at 50 degrees C for 20 min and 4.00 ml of sample in the headspace vial. The method gave good precision and showed a linear response. More than 100 VOC were identified in the fruit and juices studied by GC-MS. The method was employed to quantify ethanol, naphthalene and benzoic acid in four different species of Brazilian fruit and their juices" |
Keywords: | Anacardium/chemistry Benzoic Acid/analysis Beverages/*analysis Ethanol/analysis Flame Ionization/methods Food Analysis/methods Fruit/*chemistry Gas Chromatography-Mass Spectrometry/methods Mangifera/chemistry Naphthalenes/analysis Psidium/chemistry Volati; |
Notes: | "Medlinede Lourdes Cardeal, Zenilda Guimaraes, Eliana Moreira Parreira, Fabricio Vilela eng Research Support, Non-U.S. Gov't England 2005/07/16 Food Addit Contam. 2005 Jun; 22(6):508-13. doi: 10.1080/02652030500132893" |