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Anal Sci

Title:		Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device
Author(s):		Ueta I; Takenaka R; Fujimura K; Yoshimura T; Narukami S; Mochizuki S; Maeda T;
Address:		"Department of Applied Chemistry, University of Yamanashi, 4-3-11 Takeda, Kofu, 400-8511, Japan. iueta@yamanashi.ac.jp. Department of Applied Chemistry, University of Yamanashi, 4-3-11 Takeda, Kofu, 400-8511, Japan. Shinwa Chemical Industries Ltd., 50-2 Kagekatsu, Fushimi, Kyoto, 612-8307, Japan. HORIBA STEC, Co. Ltd., 11-5 Hokotate, Kamitoba, Minami, Kyoto, 601-8116, Japan. Professionals' Network in Advanced Instrumentation Society, 2-6 Kanda-Awaji, Chiyoda, Tokyo, 101-0063, Japan"
Journal Title:		Anal Sci
Year:		2020
Volume:		20200417
Issue:		9
Page Number:		1071 - 1074
DOI:		10.2116/analsci.20P022
ISSN/ISBN:		1348-2246 (Electronic) 0910-6340 (Linking)
Abstract:		"A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng L(-1) for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings"
Keywords:		Volatile organic compounds gas chromatography semi-volatile organic compounds sick house syndrome;
Notes:		"PubMed-not-MEDLINEUeta, Ikuo Takenaka, Risa Fujimura, Koji Yoshimura, Tomotaka Narukami, Shoji Mochizuki, Suguru Maeda, Tsuneaki eng Switzerland 2020/04/21 Anal Sci. 2020 Sep 10; 36(9):1071-1074. doi: 10.2116/analsci.20P022. Epub 2020 Apr 17"