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Anal Sci

Title:		Quantification of 23 Volatile Organic Compounds with a Single Reference Material Using Post-column Reaction Gas Chromatography Combined with a Stainless-steel Heating Furnace
Author(s):		Kitamaki Y; Saito N; Sasaki N; Morita M; Sasaki T; Miyamoto H; Numata M; Ihara T;
Address:		"National Metrology Institute of Japan (NMIJ), National Institute of Advanced Industrial Science and Technology (AIST), 1-1-1 Umezono, Tsukuba, Ibaraki, 305-8563, Japan. y-kitamaki@aist.go.jp. National Metrology Institute of Japan (NMIJ), National Institute of Advanced Industrial Science and Technology (AIST), 1-1-1 Umezono, Tsukuba, Ibaraki, 305-8563, Japan. Horiba Stec Co., Ltd., 11-5 Hokotate Kamitoba, Minami, Kyoto, 601-8116, Japan"
Journal Title:		Anal Sci
Year:		2021
Volume:		20210205
Issue:		8
Page Number:		1185 - 1188
DOI:		10.2116/analsci.20N036
ISSN/ISBN:		1348-2246 (Electronic) 0910-6340 (Linking)
Abstract:		"We built a heating furnace using stainless-steel instead of aluminum in gas chromatography combined with an oxidation/reduction system; it increased the oxidation temperature to 650 degrees C. At 600 degrees C, it completely oxidized five organochlorine compounds. This system was applied to a standard solution of 23 volatile organic compounds. The analytical results of 20 hydrocarbon and organochlorine compounds showed good agreement with the expanded uncertainty (k = 2) of the reference values. Three organobromine compounds obtained values higher than the reference; this was investigated further"
Keywords:		Post-column reaction gas chromatography organobromine compounds organochlorine compounds volatile organic compound;
Notes:		"PubMed-not-MEDLINEKitamaki, Yuko Saito, Naoki Sasaki, Nanako Morita, Mariko Sasaki, Tomohiro Miyamoto, Hideaki Numata, Masahiko Ihara, Toshihide eng Switzerland 2021/02/09 Anal Sci. 2021 Aug 10; 37(8):1185-1188. doi: 10.2116/analsci.20N036. Epub 2021 Feb 5"