| Title: | Rapid and Sensitive Analysis of Volatile Components of Different Parts of Clausena lansium by Ionic Liquid Based Headspace Gas Chromatography-Mass Spectrometry |
| Author(s): | He X; Ma Y; Yi G; Wen Y; Zhang Y; Zhang H; Zhang L; |
| Address: | "School of Pharmacy, Hebei Medical University, Shijiazhuang 050017, China. xiaowen_he@126.com. Public Research Laboratory, Hainan Medical University, Haikou 571199, China. xiaowen_he@126.com. School of Public Health, Hainan Medical University, Haikou 571199, China. hbykdxmyz@163.com. Public Research Laboratory, Hainan Medical University, Haikou 571199, China. guohuiyi6@163.com. Key Laboratory of Translation Medicine Tropical Disease, Department of Ministry of Education, Hainan Medical University, Haikou 571199, China. wyy_418@163.com. Public Research Laboratory, Hainan Medical University, Haikou 571199, China. hnmuzyx@126.com. Public Research Laboratory, Hainan Medical University, Haikou 571199, China. hyzhang_xjtu2013@aliyun.com. School of Pharmacy, Hebei Medical University, Shijiazhuang 050017, China. zhanglantong@263.net" |
| DOI: | 10.3390/molecules24010091 |
| ISSN/ISBN: | 1420-3049 (Electronic) 1420-3049 (Linking) |
| Abstract: | "A rapid and sensitive ionic liquid (IL) based headspace gas chromatography-mass spectrometry (HS-GC-MS) method was developed for analyzing volatile components in leaf, pericarp, and seed of Clausena lansium from different areas in Hainan Province, China. HS efficiencies were carefully investigated by using three ILs and water as matrix media. Extraction parameters, including equilibrium temperature, equilibrium time, and stirring rate had been evaluated and optimized by using an orthogonal design with OA(9)(3(3)) table. Under the optimized condition of IL-based HS-GC-MS, only 100 mg of sample and 2 mL of [Bmim][BF(4)] were needed to comprehensively and accurately analyze the volatile components in Clausena lansium. By utilizing a cluster analysis, six clusters were obtained for ninety components. This method was simpler, more rapid, and more sensitive when compared with previously reported methods for analyzing and identifying volatile components in Clausena lansium. The results may provide a theoretical basis for further exploitation of Clausena lansium" |
| Keywords: | Analysis of Variance Clausena/*chemistry Gas Chromatography-Mass Spectrometry/*methods Ionic Liquids/*chemistry Phylogeny Plant Leaves/chemistry Seeds/chemistry Volatile Organic Compounds/*analysis Clausena lansium cluster analysis headspace ionic liquid; |
| Notes: | "MedlineHe, Xiaowen Ma, Yinzheng Yi, Guohui Wen, Yingying Zhang, Yunxia Zhang, Haiying Zhang, Lantong eng 81660224/National Natural Science Foundation of China/ ZDYF2017120/Key R & D Project of Hainan/ Switzerland 2018/12/29 Molecules. 2018 Dec 27; 24(1):91. doi: 10.3390/molecules24010091" |
