Title: | [Determination of low concentration VOCs in air by a newly designed needle trap device] |
Address: | "Department of Environmental Science and Engineering, Fudan University, Shanghai 200433, China. lixiang@fudan.edu.cn" |
ISSN/ISBN: | 0250-3301 (Print) 0250-3301 (Linking) |
Abstract: | "Targeting on the problem of atmospheric VOCs that are presenting low concentration and difficult for sampling, a newly designed needle trap device with carboxen 1000 as a sorbent material was developed. The main advantages of needle trap device are the simple methodology,the easiness and the rapidity of the analysis coupling with GC-MS. No solvent was used in all experiments. Volatile analytes benzene, toluene, ethylbenzene and xylenes (BTEX) were chosen as target compounds to validate this device from theory to real application. The experimental parameters as breakthrough volume of stripping gas were investigated. LOD ranges was obtained at 0.05 ng x mL(-1), and the standard recovery was from 86.5% to 110.5% respectively. Needle trap device is suitable for sampling in field" |
Keywords: | Air Pollutants/*analysis Benzene/analysis Chemical Fractionation/*instrumentation/methods Gas Chromatography-Mass Spectrometry/instrumentation/*methods *Needles Toluene/analysis Volatile Organic Compounds/*analysis Xylenes/analysis; |
Notes: | "MedlineLi, Xiang Chen, Jian-Min chi English Abstract Research Support, Non-U.S. Gov't China 2012/04/04 Huan Jing Ke Xue. 2011 Dec; 32(12):3613-6" |