| Title: | Identification of volatile organic compounds emitted by a naturally aged book using solid-phase microextraction/gas chromatography/mass spectrometry |
| Author(s): | Lattuati-Derieux A; Bonnassies-Termes S; Lavedrine B; |
| Address: | "Centre de Recherches sur la Conservation des Documents Graphiques, CRCDG FRE 2743, Paris Cedex 05, France. lattuati@mnhn.fr" |
| DOI: | 10.1016/j.chroma.2003.11.069 |
| ISSN/ISBN: | 0021-9673 (Print) 0021-9673 (Linking) |
| Abstract: | Solid-phase microextraction (SPME) coupled to gas chromatography/mass spectrometry (GC/MS) has been applied to the analysis of volatile organic compounds emitted from a naturally aged groundwood pulp paper originating from an old book in order to access the products produced through the decomposition reactions occurring in paper upon ageing. Two different extraction methods were developed and compared: headspace SPME and contact SPME. The influence of few extraction parameters were tested in order to define the best extraction conditions. An optimised non-destructive contact SPME method was elaborated and allowed the characterisation of more than 50 individual constituents |
| Keywords: | *Books Gas Chromatography-Mass Spectrometry/*methods Organic Chemicals/*analysis/chemistry/*isolation & purification *Paper Temperature Time Factors Volatilization; |
| Notes: | "MedlineLattuati-Derieux, Agnes Bonnassies-Termes, Sylvette Lavedrine, Bertrand eng Netherlands 2004/02/12 J Chromatogr A. 2004 Feb 13; 1026(1-2):9-18. doi: 10.1016/j.chroma.2003.11.069" |
