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Molecules

Title:		Comparison of Extraction Techniques for the Determination of Volatile Organic Compounds in Liverwort Samples
Author(s):		Guzowska M; Wasiak W; Wawrzyniak R;
Address:		"Faculty of Chemistry, Adam Mickiewicz University in Poznan, Uniwersytetu Poznanskiego 8, 61-614 Poznan, Poland"
Journal Title:		Molecules
Year:		2022
Volume:		20220503
Issue:		9
Page Number:		-
DOI:		10.3390/molecules27092911
ISSN/ISBN:		1420-3049 (Electronic) 1420-3049 (Linking)
Abstract:		"This article focuses on the comparison of four popular techniques for the extraction of volatile organic compounds (VOCs) from liverworts of the Calypogeia azurea species. Since extraction is the most important step in the sample analysis of ingredients present in botanical preparations, their strengths, and weaknesses are discussed. In order to determine the VOCs present in plants, selecting the appropriate one is a key step of the extraction technique. Extraction should ensure the isolation of all components present in the oily bodies of Calypogeia azurea without the formation of any artifacts during treatment. The best extraction method should yield the determined compounds in detectable amounts. Hydrodistillation (HD), applying Deryng apparatus and solid-liquid extraction (SLE), microwave-assisted extraction (MAE), and headspace solid-phase microextraction (HS-SPME) were used for volatile extraction. The extracts obtained were analysed by gas chromatography coupled to mass spectrometry (GC-MS) to determine the compounds"
Keywords:		*Anemone Gas Chromatography-Mass Spectrometry/methods *Hepatophyta Solid Phase Microextraction/methods *Volatile Organic Compounds/analysis Calypogeia azurea Hepaticae Mae Sle Spme extraction hydrodistillation liverworts specialized metabolites volatile o;
Notes:		"MedlineGuzowska, Malgorzata Wasiak, Wieslaw Wawrzyniak, Rafal eng 2017/27/B/NZ8/01091/National Science Centre/ POWR.03.02.00-00-I020/17/European Union through the European Social Fund under the Operational Program Knowledge Education Development/ Switzerland 2022/05/15 Molecules. 2022 May 3; 27(9):2911. doi: 10.3390/molecules27092911"